A solution-liquid-solid approach to colloidal indium nitride nanoparticles from simple alkylamide precursors and investigation of its mechanism / by Yang Chen.
"This thesis reports a solution-based method to synthesize colloidal InN nanomaterials where InBr3 and oleylamide were employed as indium and nitrogen precursors, respectively, and its possible mechanism. Characterizations by X-ray diffraction, Raman spectroscopy, Transmission electron microscopy, X...
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| Language: | English |
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2017.
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| Dissertation Note: |
Thesis M.S. Michigan State University. Chemistry 2017 |
| Physical Description: | 1 online resource (xvii, 159 pages) : illustrations (chiefly color) |
| Format: | Thesis Electronic eBook |
MARC
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| 100 | 1 | |a Chen, Yang |c (Graduate of Michigan State University in chemistry), |e author. |0 http://id.loc.gov/authorities/names/no2019067342 | |
| 245 | 1 | 2 | |a A solution-liquid-solid approach to colloidal indium nitride nanoparticles from simple alkylamide precursors and investigation of its mechanism / |c by Yang Chen. |
| 260 | |c 2017. | ||
| 300 | |a 1 online resource (xvii, 159 pages) : |b illustrations (chiefly color) | ||
| 336 | |a text |b txt |2 rdacontent | ||
| 337 | |a computer |b c |2 rdamedia | ||
| 338 | |a online resource |b cr |2 rdacarrier | ||
| 500 | |a Electronic resource. | ||
| 502 | |g Thesis |b M.S. |c Michigan State University. Chemistry |d 2017 | ||
| 504 | |a Includes bibliographical references. | ||
| 520 | 3 | |a "This thesis reports a solution-based method to synthesize colloidal InN nanomaterials where InBr3 and oleylamide were employed as indium and nitrogen precursors, respectively, and its possible mechanism. Characterizations by X-ray diffraction, Raman spectroscopy, Transmission electron microscopy, X-ray photoelectron spectroscopy and Near infrared-visible absorption support this method as a convincing advancement toward high quality zinc-blende InN nanoparticles. Nuclear magnetic resonance and Gas chromatography were used to qualify the byproducts of this approach. A possible reaction mechanism is also proposed here: (1) NH2 - intermediate is produced as a result of the formation of the secondary imine. (2) NH2 - intermediate reacts with In3+ to form a complex which easily decomposes to produce (InN)n clusters. (3) In(0) nanoparticles produced by reduction of In3+ by H-catalyzed the formation of zinc-blende InN with high crystallinity."--Page ii. | |
| 588 | |a Description based on online resource; title from PDF title page (viewed on April 18, 2019) | ||
| 650 | 0 | |a Semiconductor nanocrystals |x Synthesis. |0 http://id.loc.gov/authorities/subjects/sh2003008302 | |
| 650 | 0 | |a Nanostructured materials |x Design and construction. |0 http://id.loc.gov/authorities/subjects/sh93000864 | |
| 650 | 0 | |a Nanoparticles |x Synthesis. |0 http://id.loc.gov/authorities/subjects/sh85089689 | |
| 655 | 0 | |a Electronic dissertations. | |
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